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Computational analysis of the influence of initial defects on the ceramic foam failure upon mechanical loading
Papšík, Roman ; Majer, Zdeněk (referee) ; Ševeček, Oldřich (advisor)
The thesis deals with computational modelling of ceramic foams and analysis of influence of structural manufacturing defects (like broken struts, closed pores and material clumps) have on foam strength. Model of foam geometry was discretized using beam elements in order to decrease computational cost. In place where several struct join, rigid beam element was used so that the increased stiffness is better modelled. Closed walls of pores were modelled and discretised by shell elements. Influence of loading direction was analysed on foams containing no defects and then influence of amount of defects in foam on strength was further analysed. Highest strength show foams created by cells whose structs are oriented in direction of loading. These were losing strength most rapidly. Foam with structure of rhombic dodecahedral cell was least influenced by presence of closed pore defects but it also showed lowest strength even without defects. Cells with struts oriented in direction of loading experienced biggest drop in strength. Kelvin cell is a compromise. It was shown that difference in strength of strut with constant and varying cross-section is tenths of percent.
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Modelling of the randomly formed ceramic foam structure for FEM simulations
Papšík, Roman ; Navrátil, Petr (referee) ; Ševeček, Oldřich (advisor)
This bachelor thesis deals with construction of ceramic foam model with various levels of (ir)regularity for finite element simulations in Ansys. The main objective is to substitute the complex structure of the open cell foam using the beam elements, enabling to perform FE analysis on much larger volumes of foams than the realistic foam models composed of solid elements. In this work, the technique of the model creation is based on the Voronoi tessellation and enables choice of arbitrary (ir)regularity of the modelled structure. The created source codes generate the model data directly in the syntax of APDL language for FEM system Ansys. The first part of the work describes several methods of the space partitioning and methods for substitution of the real foam structure by simplified “wire” model. The second part defines the Voronoi tessellation (diagram) as a key technique for creation of the foam model and describes its algorithms. The next part of the work deals with possibilities and utilizations of various software and libraries, describes creation of the own code in mathematical software Matlab and way how to transfer the model data into the system Ansys. The last part of the work demonstrates functionality of the created model on several FEM simulations, studying response of the ceramic foam on the external mechanical loading, upon consideration of various levels of the foam structure irregularity.
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Pressure loss of catalyst carriers
Linda, Matúš ; Kilkovský, Bohuslav (referee) ; Jecha, David (advisor)
The diploma thesis is divided into four main parts. The first part deals with the issue of waste management and its energy utilization in waste incineration. Processed harmful substances produced by incineration as well as emission limits. It deals with the types of catalytic carriers, their description, production and more detailed processing of ceramic foam VUKOPOR. The second part is devoted to technologies utilizing catalytic processes and a more detailed specification of the process. In the third part there is processed the calculation methods for pressure losses for individual types of carriers. Fourth, the most extensive part describes the INTEQII experimental device, its technology and construction, as well as the principle of the practical part, measuring of the pressure losses of carriers. It includes the evaluation of pressure losses in separate categories of carriers, such as the bed, HoneyComb and VUKOPOR ceramic foam. Subsequently, a comparison of the pressure losses of all carriers is made relative to the reference size of 1 m. The impact of bonding of VUKOPOR foam samples on the size of pressure losses is discussed. At the end of this section, the suitability of calculation methods for individual carriers is evaluated, depending on the experimental pressure loss data.
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Study of interaction of HA / biosklo based composites in simulated body fluid
Riša, Juraj ; Švec, Jiří (referee) ; Bartoníčková, Eva (advisor)
This work deals with bioceramic materials based of hydroxyapatite, bioglass and their composites. These materials are commonly used in medicine, especially as hard tissue substituents. They can be prepared by different types of syntheses, from which the most common were picked for this work – precipitation of hydroxyapatite and sol-gel method for bioglass. Thermal analysis and X-ray diffraction were used for characterization of prepared powders. This thesis studies mostly their features within the composite materials, which were foamed for better bone stimulation. Properties and possibility in bio application of materials is firstly studied through their interaction in simulated body fluids, which mimics ionic concentration of human plasma. Experimental part covers synthesis of ceramic powders, their characterization, preparation of mixtures and scaffolds foamed through in situ foaming, their sintering at ideal temperatures, characterization of porosity and phase changes due to sintering. Basic tests of apatite formation ability were provided by incubation of prepared scaffolds in simulated body fluid for 3, 7, 14 and 21 days and their assay in scanning electron microscopy. Changes in concentration of Ca2+ a PO4 3- ions as well as in weight of the specimen were tracked within the incubation period.
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Numerical simulation of failure of ceramic foams upon mechanical loading
Hanák, Jiří ; Skalka, Petr (referee) ; Ševeček, Oldřich (advisor)
The master’s thesis deals with a numerical simulation of failure of ceramic foams with open-cell structure and with understanding of conditions required for the failure of the structure under various mechanical loading conditions. To this purpose, the so-called stress-energy coupled criterion was utilized. The motivation for this thesis was to create a model able of the most accurate prediction of the ceramic foam strength in comparison with experimental observations. First part of the thesis is focused on the theoretical background required for solving the problem. More specifically there are mentioned methods of the foam material modelling, Linear Elastic Fracture Mechanic (LEFM) and coupled stress-energy criterion used for definition of the crack initiation. In the second part of the thesis, numerical Finite Element Analyses (FEA) whose main purpose was to determine critical conditions necessary for the initiation of strut failure within the foam structure, were performed. These pieces of knowledge were then used for creation of the numerical simulation algorithm of the mechanical test of foam material with regular cell pattern. Outputs of numerical simulations were at the end of this work compared with experimental results (of the compression test) made on the real Al_2 O_3 foams prepared by 3D printing technology and provided by the Institute of Physics of Materials Czech Academy of Science. It can be concluded that a good agreement between results of both approaches was reached and the prediction of the ceramic foam mechanical strength using the developed model is in the meanwhile the most accurate estimation from recently published approaches.
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Study of interaction of HA / biosklo based composites in simulated body fluid
Riša, Juraj ; Švec, Jiří (referee) ; Bartoníčková, Eva (advisor)
This work deals with bioceramic materials based of hydroxyapatite, bioglass and their composites. These materials are commonly used in medicine, especially as hard tissue substituents. They can be prepared by different types of syntheses, from which the most common were picked for this work – precipitation of hydroxyapatite and sol-gel method for bioglass. Thermal analysis and X-ray diffraction were used for characterization of prepared powders. This thesis studies mostly their features within the composite materials, which were foamed for better bone stimulation. Properties and possibility in bio application of materials is firstly studied through their interaction in simulated body fluids, which mimics ionic concentration of human plasma. Experimental part covers synthesis of ceramic powders, their characterization, preparation of mixtures and scaffolds foamed through in situ foaming, their sintering at ideal temperatures, characterization of porosity and phase changes due to sintering. Basic tests of apatite formation ability were provided by incubation of prepared scaffolds in simulated body fluid for 3, 7, 14 and 21 days and their assay in scanning electron microscopy. Changes in concentration of Ca2+ a PO4 3- ions as well as in weight of the specimen were tracked within the incubation period.
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Numerical simulation of failure of ceramic foams upon mechanical loading
Hanák, Jiří ; Skalka, Petr (referee) ; Ševeček, Oldřich (advisor)
The master’s thesis deals with a numerical simulation of failure of ceramic foams with open-cell structure and with understanding of conditions required for the failure of the structure under various mechanical loading conditions. To this purpose, the so-called stress-energy coupled criterion was utilized. The motivation for this thesis was to create a model able of the most accurate prediction of the ceramic foam strength in comparison with experimental observations. First part of the thesis is focused on the theoretical background required for solving the problem. More specifically there are mentioned methods of the foam material modelling, Linear Elastic Fracture Mechanic (LEFM) and coupled stress-energy criterion used for definition of the crack initiation. In the second part of the thesis, numerical Finite Element Analyses (FEA) whose main purpose was to determine critical conditions necessary for the initiation of strut failure within the foam structure, were performed. These pieces of knowledge were then used for creation of the numerical simulation algorithm of the mechanical test of foam material with regular cell pattern. Outputs of numerical simulations were at the end of this work compared with experimental results (of the compression test) made on the real Al_2 O_3 foams prepared by 3D printing technology and provided by the Institute of Physics of Materials Czech Academy of Science. It can be concluded that a good agreement between results of both approaches was reached and the prediction of the ceramic foam mechanical strength using the developed model is in the meanwhile the most accurate estimation from recently published approaches.
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Computational analysis of the influence of initial defects on the ceramic foam failure upon mechanical loading
Papšík, Roman ; Majer, Zdeněk (referee) ; Ševeček, Oldřich (advisor)
The thesis deals with computational modelling of ceramic foams and analysis of influence of structural manufacturing defects (like broken struts, closed pores and material clumps) have on foam strength. Model of foam geometry was discretized using beam elements in order to decrease computational cost. In place where several struct join, rigid beam element was used so that the increased stiffness is better modelled. Closed walls of pores were modelled and discretised by shell elements. Influence of loading direction was analysed on foams containing no defects and then influence of amount of defects in foam on strength was further analysed. Highest strength show foams created by cells whose structs are oriented in direction of loading. These were losing strength most rapidly. Foam with structure of rhombic dodecahedral cell was least influenced by presence of closed pore defects but it also showed lowest strength even without defects. Cells with struts oriented in direction of loading experienced biggest drop in strength. Kelvin cell is a compromise. It was shown that difference in strength of strut with constant and varying cross-section is tenths of percent.
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Pressure loss of catalyst carriers
Linda, Matúš ; Kilkovský, Bohuslav (referee) ; Jecha, David (advisor)
The diploma thesis is divided into four main parts. The first part deals with the issue of waste management and its energy utilization in waste incineration. Processed harmful substances produced by incineration as well as emission limits. It deals with the types of catalytic carriers, their description, production and more detailed processing of ceramic foam VUKOPOR. The second part is devoted to technologies utilizing catalytic processes and a more detailed specification of the process. In the third part there is processed the calculation methods for pressure losses for individual types of carriers. Fourth, the most extensive part describes the INTEQII experimental device, its technology and construction, as well as the principle of the practical part, measuring of the pressure losses of carriers. It includes the evaluation of pressure losses in separate categories of carriers, such as the bed, HoneyComb and VUKOPOR ceramic foam. Subsequently, a comparison of the pressure losses of all carriers is made relative to the reference size of 1 m. The impact of bonding of VUKOPOR foam samples on the size of pressure losses is discussed. At the end of this section, the suitability of calculation methods for individual carriers is evaluated, depending on the experimental pressure loss data.
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Fracture-mechanics behaviour of ceramic foam with macroscopic stress concentrator upon the tensile test
Ševeček, O. ; Majer, Z. ; Bertolla, Luca ; Chlup, Zdeněk ; Kotoul, M.
The work investigates an influence of the macroscopic stress concentrator inside the ceramic open cell foam structure on the fracture-mechanics response of the foam upon the tensile test. As the concentrator, the central crack/rectangular notch was taken into account. The influence of the crack/notch length and width on the stress concentration ahead the concentrator tip was assessed using the simplified FE beam element based model with irregular cells simulating the real ceramic foam structure. Average principal stresses calculated on set of struts ahead the crack/notch tip were compared with average stresses in the intact structure. It was found that the ratio of these stresses increases linearly with the crack length. The stress concentration ratio is slightly lower in case of thick rectangular notch than in case of a thin crack. Furthermore, the failure load leading to complete fracture of the studied specimens, subjected to the tensile loading, were calculated using the same model. It is shown that the difference factor between the critical fracture force in case of structure without concentrator and with concentrator is very close to the concentration factor calculated from the average stresses on particular struts in the region in front of the concentrator tip.\n
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